HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 117920672, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 89881737 | HCID 89881737 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 117920672 | HCID 117920672 | — |
Reaction Steps
In addition, the low-melting point crystals Compound 21 were dissolved in methylene chloride, and treated with hydrogen chloride-dioxane, to produce 3-[4((E)-2-decenoyl)piperazin-1-yl]propionic acid hydrochloride (crystals, mp 201°-203° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09428477B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-878b18de57e14e658572d37972099d7d |
| Source note | uspto-grants-2016_08 |