HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67085866, compound → HCID 18353825, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67085866 | HCID 67085866 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18353825 | HCID 18353825 | 95.6% |
Reaction Steps
A solution of benzyl 5-isopropenylpicolinate (1.27 g, 5 mmol) in MeOH (25 mL) was subjected to hydrogenation with 20% Pd(OH)2/C (200 mg) with a H2 balloon for 2 h. The product 5-isopropenylpicolinic acid (780 mg) was obtained by filtration and concentration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09428475B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-ec108bedbd4044bd8d5bcf263e895630 |
| Source note | uspto-grants-2016_08 |