Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
n-Cyclohexylpiperidine-4-carboxamide → HCID 86706526, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | n-Cyclohexylpiperidine-4-carboxamide | HCID 12410238 | — |
| 반응물 | 2-Chloro-3-nitrobenzaldehyde | HCID 12667713 | — |
| 반응물 | 1-(2-Chloro-3-nitro-benzyl)-piperidine-4-carboxylic acid cyclohexylamide | HCID 86706527 | — |
| 생성물 | HCID 86706526 | HCID 86706526 | — |
반응 단계
The title compound is prepared according to the reactions described above starting from 2-chloro-3-nitro-benzaldehyde and piperidine-4-carboxylic acid cyclohexylamide giving after reductive amination 1-(2-chloro-3-nitro-benzyl)-piperidine-4-carboxylic acid cyclohexylamide LC-MS B: tR=0.57 min; [M+H]+=380.14 and reduction with stannous chloride the title compound LC-MS A: tR=0.50 min; [M+H]+=350.20.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09428456B2 |
| 출처 데이터셋 | uspto-grants-2016_08 |
| ORD ID | ord-f2b5c8cf9e8b451690eb334efb45e56a |
| 출처 메모 | uspto-grants-2016_08 |