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HRID1486700

反应详情

EQUATION

反应方程式

HRID 1486700 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)NC(=O)C1CCNCC1
HCID7175833

未命名化合物

结构：O=Cc1cc(Br)cc([N+](=O)[O-])c1
HCID16743966

3-Bromo-5-nitrobenzaldehyde

C7H4BrNO3

PRODUCTS

生成物

1
结构：CC(C)(C)NC(=O)C1CCN(Cc2cc(N)cc(Br)c2)CC1
HCID86706532

未命名化合物

PROCEDURE

实验过程

The title compound is prepared according to the reactions described above starting from 3-bromo-5-nitro-benzaldehyde and piperidine-4-carboxylic acid tert-butylamide yielding after reductive amination BB-10a; LC-MS A: tR=0.65 min; [M+H]+=398.00 followed by reduction with stannous chloride the title compound; LC-MS A: tR=0.60 min; [M+H]+=369.67.

WORKUP

后处理

  1. customThe title compound is prepared