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HRID1486704

反应详情

EQUATION

反应方程式

HRID 1486704 的结构方程式

REACTANTS

反应物

3
结构：CC(C)(C)NC(=O)C1CCNCC1
HCID7175833

未命名化合物

结构：Cc1ccc([N+](=O)[O-])cc1C=O
HCID12654145

2-Methyl-5-nitrobenzaldehyde

C8H7NO3

结构：Cc1ccc([N+](=O)[O-])cc1CN1CCC(C(=O)NC(C)(C)C)CC1
HCID86706536

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(N)cc1CN1CCC(C(=O)NC(C)(C)C)CC1
HCID86706535

未命名化合物

PROCEDURE

实验过程

The title compound is prepared according to the reactions described for BB-5 above starting from 2-methyl-5-nitro-benzaldehyde and piperidine-4-carboxylic acid tert-butylamide yielding after reductive amination 1-(2-methyl-5-nitro-benzyl)-piperidine-4-carboxylic acid tert-butylamide; LC-MS A: tR=0.62 min; [M+H]+=334.21 followed by reduction with stannous chloride the title compound; LC-MS A: tR=0.44 min; [M+H]+=304.28.

WORKUP

后处理

  1. customThe title compound is prepared