HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Fluoropyridine-2-carbonyl chloride → 5-Fluoro-pyridine-2-carboxylic acid (3-[1,3]dioxolan-2-yl-phenyl)-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Fluoropyridine-2-carbonyl chloride | HCID 21942698 | — |
| Reactant | N-(3-[1,3]Dioxolan-2-yl-phenyl)-5-methyl-nicotinamide | HCID 86706559 | — |
| Product | 5-Fluoro-pyridine-2-carboxylic acid (3-[1,3]dioxolan-2-yl-phenyl)-amide | HCID 131736815 | — |
Reaction Steps
The subtitle compound is prepared according to the reaction 4.01a described above using 5-fluoropicolinoyl chloride: LC-MS A: tR=0.89 min; [M+H]+=289.29.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09428456B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-512f412116204f64b59a43b7c42f6a65 |
| Source note | uspto-grants-2016_08 |