HRID1486862

反应详情

EQUATION

反应方程式

HRID 1486862 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2,2′-(3-(3-((4-Carbamimidamidobenzoyl)oxy)phenyl)-4,5-dihydro-1,2-oxazole-5,5-diyl)diacetic acid trifluoroacetate (40.9 mg) was suspended in water (1 mL), and an aqueous solution prepared from ammonium acetate (17.06 mg) and water (1 mL) was added to the suspension at room temperature. The obtained mixture was stirred at room temperature for 1 hour, and then, the solid was collected by filtration and washed with water and acetone to obtain the title compound (28.4 mg).

WORKUP

后处理

  1. additionwas added to the suspension at room temperature
  2. filtrationthe solid was collected by filtration
  3. washwashed with water and acetone