HRID1486877

反应详情

EQUATION

反应方程式

HRID 1486877 的结构方程式

PROCEDURE

实验过程

A mixture of tert-butyl 5-(2-tert-butoxy-2-oxoethyl)-3-(5-((4-carbamimidamidobenzoyl)oxy)-2-cyclohexylphenyl)-4,5-dihydro-1,2-oxazole-5-carboxylate (12.7 mg) and TFA (1 mL) was stirred at room temperature for 2 hours. The reaction mixture was concentrated under reduced pressure, and then, the residue was washed with diethyl ether to obtain the title compound (5.8 mg).

WORKUP

后处理

  1. concentrationThe reaction mixture was concentrated under reduced pressure
  2. washthe residue was washed with diethyl ether