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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1487123Generated: November 2, 2026

Triethylsilane → HCID 16792092, compound

https://huagongshe.com/reaction/1487123

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylsilaneHCID 12052—
ReactantHCID 9245646HCID 9245646—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 16792092HCID 16792092—

Reaction Steps

To a stirred solution of (4-hydroxypiperidin-1-yl)(3-nitrophenyl)methanone (1 g, 4.00 mmol) and Pd—C (10%, 0.425 g,) in Methanol (10 ml) was added triethylsilane (3.19 ml, 19.98 mmol) dropwise at room temperature. The reaction mixture was filtered through celite bed. The filtrate was concentrated under vacuum to give the title compound. (0.8 gm)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09428499B2
Source datasetuspto-grants-2016_08
ORD IDord-115be414f9c045d080c20f54f1b16433
Source noteuspto-grants-2016_08