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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1487125Generated: November 1, 2026

HCID 80107846, compound → HCID 80108036, compound

https://huagongshe.com/reaction/1487125

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 80107846HCID 80107846—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 80108036HCID 8010803692.5%

Reaction Steps

To a stirred solution of 3-Nitro-N-(oxetan-3-yl)benzamide (0.06 g, 0.270 mmol) in methanol (5 ml) was added Pd/C (2.87 mg) and the reaction mixture was stirred under hydrogen atmosphere for 20 min. The reaction mixture was diluted with methanol (10 ml) and the mixture was filtered through celite, and the filtrate was concentrated under vacuum to afford the title compound (48 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09428499B2
Source datasetuspto-grants-2016_08
ORD IDord-8d514fff05fe4afcab73060429d99e1e
Source noteuspto-grants-2016_08