HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 80107846, compound → HCID 80108036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 80107846 | HCID 80107846 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 80108036 | HCID 80108036 | 92.5% |
Reaction Steps
To a stirred solution of 3-Nitro-N-(oxetan-3-yl)benzamide (0.06 g, 0.270 mmol) in methanol (5 ml) was added Pd/C (2.87 mg) and the reaction mixture was stirred under hydrogen atmosphere for 20 min. The reaction mixture was diluted with methanol (10 ml) and the mixture was filtered through celite, and the filtrate was concentrated under vacuum to afford the title compound (48 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09428499B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-8d514fff05fe4afcab73060429d99e1e |
| Source note | uspto-grants-2016_08 |