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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1487133Generated: October 31, 2026

HCID 89828081, compound → HCID 89828080, compound

https://huagongshe.com/reaction/1487133

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 89828081HCID 89828081—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 89828080HCID 8982808078.7%

Reaction Steps

1-(Azetidin-1-yl)-2-(3-nitrophenyl)ethanone (0.5 g, 2.27 mmol) was taken in methanol (20 ml) and at 0° C., Pd—C (10%, 0.05 g) was added. The reaction mixture was stirred under hydrogen atmosphere at room temperature for 5 hrs. The reaction mixture was filtered through celite and the filtrate was concentrated under vacuum to afford the title product (0.34 gm).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09428499B2
Source datasetuspto-grants-2016_08
ORD IDord-aaf26266adbe45768784972f8776954c
Source noteuspto-grants-2016_08