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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1487135Generated: November 2, 2026

HCID 89815274, compound → HCID 80108274, compound

https://huagongshe.com/reaction/1487135

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 89815274HCID 89815274—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 80108274HCID 8010827496.5%

Reaction Steps

2-(3-Nitrophenyl)-N-(oxetan-3-yl)acetamide (0.5 g, 2.11 mmol) was taken in methanol (20 ml) and at 0° C., 10% Pd—C (0.5 g) was added. The reaction mixture was stirred under hydrogen atmosphere at room temperature for 5 hrs. The reaction mixture was filtered through celite and the filtrate was concentrated under vacuum to afford the title product (0.42 gm).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09428499B2
Source datasetuspto-grants-2016_08
ORD IDord-4596d39689fc4d45b7be6c918e725d2d
Source noteuspto-grants-2016_08