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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1487137Generated: November 1, 2026

HCID 89828092, compound → HCID 89828093, compound

https://huagongshe.com/reaction/1487137

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 89828092HCID 89828092—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 89828093HCID 8982809396.2%

Reaction Steps

1-(3-hydroxyazetidin-1-yl)-2-(3-nitrophenyl)ethanone (0.5 g, 2.117 mmol) was taken in methanol (20 ml) and at 0° C., Pd—C (10%, 0.5 g) was added. The reaction mixture was stirred under hydrogen atmosphere at room temperature for 5 hrs. The reaction mixture was filtered through celite and the filtrate was concentrated under vacuum to afford the title product (0.42 gm).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09428499B2
Source datasetuspto-grants-2016_08
ORD IDord-5c9f3df46b0e452ba0268057cc5e3227
Source noteuspto-grants-2016_08