HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 89815500, compound → HCID 89815390, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 89815500 | HCID 89815500 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 89815390 | HCID 89815390 | 81.2% |
Reaction Steps
To the suspension of N-(1-carbamoylcyclopropyl)-3-nitrobenzamide (0.28 g, 1.123 mmol) in methanol (5 ml), Pd—C (0.05 g) was added under nitrogen and stirred the reaction mixture under hydrogen atmosphere at room temperature. After 2 hr, reaction mixture was filtered and concentrated under vacuum to afford solid compound (0.2 g, 81%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09428499B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-2a8f3d11add44893b0778a8a229e104b |
| Source note | uspto-grants-2016_08 |