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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1487141Generated: November 1, 2026

HCID 89815500, compound → HCID 89815390, compound

https://huagongshe.com/reaction/1487141

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 89815500HCID 89815500—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 89815390HCID 8981539081.2%

Reaction Steps

To the suspension of N-(1-carbamoylcyclopropyl)-3-nitrobenzamide (0.28 g, 1.123 mmol) in methanol (5 ml), Pd—C (0.05 g) was added under nitrogen and stirred the reaction mixture under hydrogen atmosphere at room temperature. After 2 hr, reaction mixture was filtered and concentrated under vacuum to afford solid compound (0.2 g, 81%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09428499B2
Source datasetuspto-grants-2016_08
ORD IDord-2a8f3d11add44893b0778a8a229e104b
Source noteuspto-grants-2016_08