HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86726494, compound → HCID 86726495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86726494 | HCID 86726494 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86726495 | HCID 86726495 | 94% |
Reaction Steps
To a solution of (R)-(3-methoxy-4-nitrophenyl)(2-methylaziridin-1-yl)methanone (1 equiv) in MeOH (0.22 M) was added 10% palladium on carbon (18 weight %). The reaction was stirred at room temperature for 1 h under hydrogen. The mixture was filtered through a pad of celite and concentrated to give the desired product (94% yield) as a white solid. MS (ESI) m/z 207.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09428509B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-a543489794f948599de701e3a7312884 |
| Source note | uspto-grants-2016_08 |