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HRID1487940

反应详情

EQUATION

反应方程式

HRID 1487940 的结构方程式

REACTANTS

反应物

2
结构：C[Si](C)(C)C#Cc1ccc(Br)cc1
HCID4226980

(4-Bromophenylethynyl)trimethylsilane

C11H13BrSi

2 次

结构：CC(C)(C)OC(=O)N1CCC(c2ccc3[nH]ncc3c2)CC1
HCID49760224

tert-Butyl 4-(1H-indazol-5-yl)piperidine-1-carboxylate

C17H23N3O2

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCC(c2ccc(C#C[Si](C)(C)C)cc2)CC1
HCID59805220

未命名化合物

收率 67%

PROCEDURE

实验过程

The title compound was prepared using standard chemical manipulations and procedures similar to those used for the preparation of compound 62.4, except ((4-bromophenyl)ethynyl)trimethylsilane (compound 76.1, 850 mg, 3.36 mmol) was used in place of 5-bromo-1H-indazole to yield the title compound as a yellow oil (0.80 g, 67%).

WORKUP

后处理

  1. customThe title compound was prepared