HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1488186Generated: November 3, 2026
Acetic Acid Mixture with Hydrobromic Acid → HCID 178424692, compound
https://huagongshe.com/reaction/1488186
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid Mixture with Hydrobromic Acid | HCID 21893785 | — |
| Reactant | HCID 178494727 | HCID 178494727 | — |
| Product | HCID 178424692 | HCID 178424692 | 90% |
Reaction Steps
A mixture of methyl 5-(4-chloro-3-(methoxymethyl)-1H-pyrazol-5-yl)-2,4-dimethylbenzoate (compound 281.3, 20 mg, 0.06 mmol) and HBr-HOAc (5 mL) was stirred overnight at 80° C., then concentrated under reduced pressure to yield 20 mg (90%) of the title compound as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09428502B2 |
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| Source dataset | uspto-grants-2016_08 |
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| ORD ID | ord-4a6ba192ac89418bacdbed7145cc9d4d |
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| Source note | uspto-grants-2016_08 |
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