HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Sulfite → Sodium 4-benzyloxyphenethyl sulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Sulfite | HCID 24437 | — |
| Reactant | 1-(Benzyloxy)-4-(2-bromoethyl)benzene | HCID 16638827 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | tert-Butanol | HCID 6386 | — |
| Product | Sodium 4-benzyloxyphenethyl sulfonate | HCID 86751366 | — |
Reaction Steps
A mixture of 4-benzyloxyphenethyl bromide (11.8 g) and sodium sulfite (8.91 g) in tert-butyl alcohol (40 ml) and water (80 ml) is heated at reflux for 40 hours, cooled to room temperature, filtered and the solid washed with water and ether to give sodium 4-benzyloxyphenethyl sulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05674482 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-124122ce245f4bb1baab17b15b92627f |
| Source note | uspto-grants-1997_10 |