HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-benzyloxyphenethyl sulfonate → Ethyl 4-hydroxyphenethyl sulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-benzyloxyphenethyl sulfonate | HCID 22904628 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Ethyl 4-hydroxyphenethyl sulfonate | HCID 22904632 | — |
Reaction Steps
To a solution of ethyl 4-benzyloxyphenethyl sulfonate (1.43 g) in ethyl acetate (25 ml) is added 10% palladium on carbon (0.25 g) and the mixture shaken under 30 psi of hydrogen for 3 hours. The mixture is filtered and concentrated in vacuo to give ethyl 4-hydroxyphenethyl sulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05674482 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-8aabc9ad8e5c4f8889a411bd917c1cb5 |
| Source note | uspto-grants-1997_10 |