Hydrogen Bromide → HCID 70192082, compound
Reaction equation
[NH2:1][CH2:2][CH2:3][C:4]1[CH:14]=[CH:13][C:7]2[N:8]=[C:9]([O:11]C)[S:10][C:6]=2[CH:5]=1.[BrH:15]>>[BrH:15].[NH2:1][CH2:2][CH2:3][C:4]1[CH:14]=[CH:13][C:7]2[NH:8][C:9](=[O:11])[S:10][C:6]=2[CH:5]=1Participants
3
Procedure
The resultant 6-(2-aminoethyl)-2-methoxy-1,3-benzothiazole (1.3 g) was dissolved in 48% HBr (9 ml) and the reaction mixture was stirred under reflux for 1 hour.
Workup
- temperatureunder reflux for 1 hour
Sources & evidence
- ORD record
- ord-6d9d8eac40e7477dba2a9fb09fd075cc
- Source dataset
- uspto-grants-1997_10
- Patent number
- US05674909
Reaction notes
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