Methyl Methacrylate → HCID 86750009, compound

HRID 1488917Notes

Reaction equation

HRID 1488917 reaction equation
[C:1]([O:6][CH3:7])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:8]([O:13][CH2:14][CH:15]1[O:17][CH2:16]1)(=[O:12])[C:9]([CH3:11])=[CH2:10].[C:18]([O:23][CH2:24][CH2:25][OH:26])(=[O:22])[C:19]([CH3:21])=[CH2:20]>>[C:1]([O:6][CH3:7])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:8]([O:13][CH2:14][CH:15]1[O:17][CH2:16]1)(=[O:12])[C:9]([CH3:11])=[CH2:10].[C:18]([O:23][CH2:24][CH2:25][OH:26])(=[O:22])[C:19]([CH3:21])=[CH2:20]

Participants

4

Reactant 3

HCID 6658Methyl MethacrylateHCID 7837Glycidyl methacrylateHCID 133602-Hydroxyethyl Methacrylate

Product 1

HCID 86750009HCID 86750009, compound

Procedure

Using methyl methacrylate (35.0 g, 0.35 mole), glycidyl methacrylate (28.4 g, 0.2 mole) and 2-hydroxyethyl methacrylate (13.0 g, 0.1 mole), the polymerization was carried out in the same manner as described in Synthesis Example 12, (1), and the precipitate was filtered and dried under reduced pressure to give 70.3 g of poly(methyl methacrylate/glycidyl methacrylate/2-hydroxyethyl methacrylate) as white powders having Mw 35000 and Mn 192000 (GPC with polystyrene calibration).

Workup

  1. customas described in Synthesis Example 12, (1),
  2. filtrationthe precipitate was filtered
  3. customdried under reduced pressure

Sources & evidence

ORD record
ord-0c38098e70da417daa88354498885fb0
Source dataset
uspto-grants-1997_10
Patent number
US05677112

Reaction notes

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