HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Bromoethoxy)-4-fluorobenzene → HCID 22903437, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Bromoethoxy)-4-fluorobenzene | HCID 2064171 | — |
| Reactant | tert-Butyl Dimethylphosphonoacetate | HCID 4564495 | — |
| Product | HCID 22903437 | HCID 22903437 | 61.6% |
Reaction Steps
20.5 g of tert-butyl dimethylphosphonoacetate were reacted with 25 g of 4-fluorophenoxyethyl bromide by the method described in Example 5 A). The reaction mixture was worked up as described in Example 5 A). 20.4 g of tert-butyl 4-(4-fluorophenoxy)-2-(dimethylphosphono)-n-butyrate were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05677297 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-45d0f7d8b9bb42f59a1024bfc3f3b33d |
| Source note | uspto-grants-1997_10 |