HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 22903581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 22903589 | HCID 22903589 | — |
| Reactant | HCID 178526806 | HCID 178526806 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 22903581 | HCID 22903581 | 91% |
Reaction Steps
First, 803 mg of 7-fluoro-6-nitro-1-(n-propyl)-1,4-dihydroquinoxaline-2,3-dione, 700 mg of 3-nitro-4-hydroxypyridine, and 365 mg of potassium hydroxide were allowed to react at 130° C. for 4.5 hours in dry dimethylsulfoxide in the same way as in Example 9 to give 1.059 g of 6-nitro-7-(3-nitro-4-oxo-4H-pyridin-1-yl)-1-(n-propyl)-1,4-dihydroquinoxaline-2,3-dione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05677305 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-189ebdb7341d4c39b6742186d3465c5a |
| Source note | uspto-grants-1997_10 |