HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-1,3-oxazole → HCID 22099715, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-1,3-oxazole | HCID 13371074 | — |
| Reactant | HCID 22100000 | HCID 22100000 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22099715 | HCID 22099715 | — |
Reaction Steps
To a suspension of 6-(2-methylbenzoylamino)nicotinic acid (0.3 g) in dimethylformamide (0.5 ml) and dichloromethane (2.5 ml) is added dropwise oxazolyl chloride (0.2 ml), and the mixture is stirred at room temperature for 2 hours. The mixture is evaporated under reduced pressure to remove the solvent to give 6-(2-methylbenzoylamino)nicotinoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05677299 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-3f726e84d5534d528eb64149da3cdc36 |
| Source note | uspto-grants-1997_10 |