HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → Ethyl 2-formylbenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Phthalaldehydic acid | HCID 8406 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methyl 2-formylbenzoate | HCID 243003 | — |
| Product | Ethyl 2-formylbenzoate | HCID 10943020 | — |
Reaction Steps
Using the same procedure as for the preparation of 2-carbomethoxybenzaldehyde (Compound 43), but instead using 5.0 g (33 mmol) of 2-carboxybenzaldehyde, 23.4 g (150 mmol) of iodoethane and 13.8 g (100 mmol) of K2CO3 gave the title compound as a clear colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05677320 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-4e6eba2c1a244593a6ecb9075c7f9fcb |
| Source note | uspto-grants-1997_10 |