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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1489162Generated: October 30, 2026

Hydrazine hydrate (1:1) → HCID 22903654, compound

https://huagongshe.com/reaction/1489162

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazine hydrate (1:1)HCID 24654—
ReactantHCID 22903694HCID 22903694—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 22903654HCID 22903654—

Reaction Steps

1-Benzyl-3-(dibenzylaminomethyl)-3-fluoromethylpyrrolidine (4.55 g) was dissolved in ethanol (40 ml), and 10% palladium-carbon (1 g) and hydrazine monohydrate (2.15 g) were added. The mixture was refluxed for 1 hour. After the completion of the reaction, the catalyst was removed, and the mixture was concentrated to give the object compound as an oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05677316
Source datasetuspto-grants-1997_10
ORD IDord-30b3723d6fbf4e42bc4f62d496dad0e0
Source noteuspto-grants-1997_10