HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 22878316, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 54037330 | HCID 54037330 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 22878316 | HCID 22878316 | — |
Reaction Steps
About 0.39 g sodium borohydride was added to a cold (ice bath) stirred, mixture of 3.17 g of 3'-O-acetyl-5'-carbomethoxymethylene-5'-deoxythymidine in 95 ml isopropanol. The mixture was stirred at 0° C. under nitrogen atmosphere for half an hour, then at room temperature for an additional four and one half hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05677439 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-cfdb019607f04c6ca6ae8c52676c4dc7 |
| Source note | uspto-grants-1997_10 |