1,8-Diazabicyclo(5.4.0)undec-7-ene → HCID 22904275, compound

HRID 1489466Notes

Reaction equation

HRID 1489466 reaction equation
C([O:4][CH:5]1[O:9][CH:8]([N:10]2[CH:15]=[C:14]([CH3:16])[C:13](=[O:17])[NH:12][C:11]2=[O:18])[CH2:7][CH:6]1[Si:19]([C:32]([CH3:35])([CH3:34])[CH3:33])([C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1)[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)(=O)C.C1CCN2C(=NCCC2)CC1>>[OH:4][CH:5]1[O:9][CH:8]([N:10]2[CH:15]=[C:14]([CH3:16])[C:13](=[O:17])[NH:12][C:11]2=[O:18])[CH2:7][CH:6]1[Si:19]([C:32]([CH3:35])([CH3:34])[CH3:33])([C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)[C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1

Participants

3

Reactant 2

HCID 811841,8-Diazabicyclo(5.4.0)undec-7-eneHCID 18704066HCID 18704066, compound

Product 1

HCID 22904275HCID 22904275, compound

Procedure

Compound 97 is treated as per the protocol of Baptistella et. al., Synthesis 1989, 436 with DBU to give the title compound, 98.

Sources & evidence

ORD record
ord-f68274c40b484b74a205cf78431c0efb
Source dataset
uspto-grants-1997_10
Patent number
US05677437

Reaction notes

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