HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Methyl 3-acetyl-5-bromo-4-methoxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methyl 3-acetyl-5-bromo-4-hydroxybenzoate | HCID 15818980 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Methyl 3-acetyl-5-bromo-4-methoxybenzoate | HCID 22101060 | — |
Reaction Steps
1 eq. of methyl 3-acetyl-5-bromo-4-hydroxybenzoate (preparation, see Example 19) was reacted, in acetone, with 2.0 eq. of K2CO3 and 2.1 eq. of methyl iodide to give methyl 3-acetyl-5-bromo-4-methoxybenzoate. Colorless oil, MS (ES): 288 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05679712 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-c69c1bbbd2a54f01ad510a4f1af6164e |
| Source note | uspto-grants-1997_10 |