HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → 1-Propanol, 3-(triethoxysilyl)-, 1-acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 3-(Triethoxysilyl)propyl prop-2-enoate | HCID 11119352 | — |
| Product | 1-Propanol, 3-(triethoxysilyl)-, 1-acetate | HCID 10978339 | 41% |
Reaction Steps
The same procedure as in Example 1 was followed to conduct a reaction, except that p-toluenesulfonic acid was used in place of Ti(OBu)4. After completion of the reaction, the reaction product was analyzed by GC. As a result, it was thus found that triethoxysilylpropyl acrylate as the objective compound had been obtained in a yield of 41% (in terms of triethoxysilylpropyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05679821 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-4b2e15072b7144e395dec32d4c970606 |
| Source note | uspto-grants-1997_10 |