Guaiacol → 1-Propanol, 3-(triethoxysilyl)-, 1-acetate

HRID 1489886Notes

Reaction equation

HRID 1489886 reaction equation
COC1C=CC=CC=1O.[C:10]([O:14][CH2:15][CH2:16][CH2:17][Si:18]([O:25][CH2:26][CH3:27])([O:22][CH2:23][CH3:24])[O:19][CH2:20][CH3:21])(=[O:13])[CH:11]=C>>[C:10]([O:14][CH2:15][CH2:16][CH2:17][Si:18]([O:22][CH2:23][CH3:24])([O:19][CH2:20][CH3:21])[O:25][CH2:26][CH3:27])(=[O:13])[CH3:11]

Participants

3

Reactant 2

HCID 460GuaiacolHCID 111193523-(Triethoxysilyl)propyl prop-2-enoate

Product 1

HCID 109783391-Propanol, 3-(triethoxysilyl)-, 1-acetateYield 96%

Procedure

The same procedure as in Example 1 was followed to conduct a reaction, except that 0.02 g of methoxyphenol was further added. After completion of the reaction, the reaction product was analyzed by GC. As a result, it was thus found that triethoxysilylpropyl acrylate as the objective compound had been obtained in a yield of 96% (in terms of triethoxysilylpropyl acetate).

Workup

  1. customa reaction
  2. customAfter completion of the reaction

Sources & evidence

ORD record
ord-c52eadebedba4edea8341d6d69606eb9
Source dataset
uspto-grants-1997_10
Patent number
US05679821

Reaction notes

Loading…