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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1489922Generated: October 30, 2026

2,4,6-Trimethylbenzaldehyde → HCID 86749382, compound

https://huagongshe.com/reaction/1489922

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,4,6-TrimethylbenzaldehydeHCID 10254—
ReactantDiphenylphosphine oxideHCID 254003—
ReactantSodium MethoxideHCID 10942334—
SolventTolueneHCID 1140—
ProductHCID 86749382HCID 8674938298%

Reaction Steps

To 101 g (0.5 mol) of diphenyl phosphine oxide and 74 g (0.5 mol) of 2,4,6-trimethylbenzaldehyde in 150 mL of toluene there were added 0.5 g of a 30 wt % strength sodium methylate solution. The product began to crystallize after 10 minutes and was isolated in the usual manner. Yield: 98%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05679863
Source datasetuspto-grants-1997_10
ORD IDord-164c2dcd289a41adad9c139e59ce239d
Source noteuspto-grants-1997_10