HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethane, 2-bromo-1,1-diethoxy- → HCID 178501172, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethane, 2-bromo-1,1-diethoxy- | HCID 74852 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 53999350 | HCID 53999350 | — |
| Reactant | HCID 54263894 | HCID 54263894 | — |
| Solvent | Cyclohexane ethylacetate | HCID 21867204 | — |
| Product | HCID 178501172 | HCID 178501172 | — |
Reaction Steps
The N-(2,2-diethoxyethyl)-4-(1-trifluoroacetyl-4-piperidinyl)-aniline use as amine [Rf value: 0.90 (silica gel; cyclohexane/ethyl acetate=1:3] is obtained by reacting 4-(1-trifluoroacetyl-4-piperidinyl)-aniline with bromoacetaldehyde-diethylacetal in the presence of N-ethyl-diisopropylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05681841 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-12840f38ea624693874165599391aa6d |
| Source note | uspto-grants-1997_10 |