HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21481014, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21481001 | HCID 21481001 | — |
| Product | HCID 21481014 | HCID 21481014 | — |
Reaction Steps
A 2N hydrochloric acid solution of 53.0 g of 2-[2-(2-acetamidoethyl)-4,5-dimethoxyphenyl]-5,6-dimethoxy-1-methylindole was heated under reflux for 17 hours. The reaction mixture was azeotropically distilled under reduced pressure with ethanol and benzene, and the residue was recrystallized from ethanol to yield 48 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05681954 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-d95c82e77ce549719585bdda4a2d1391 |
| Source note | uspto-grants-1997_10 |