HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 53666096, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-Acetylamino-indan-5-yl-3-pyridyl ketone | HCID 54489147 | — |
| Product | HCID 53666096 | HCID 53666096 | — |
Reaction Steps
51 g of 2-acetylamino-indan-5-yl-3-pyridyl ketone are refluxed for 16 hours with 250 ml of half concentrated hydrochloric acid. The solution is concentrated and then adjusted to pH 12 using 15N sodium hydroxide solution. The precipitate formed is washed with water and recrystallised from 100 ml of isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05681961 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-5cf9a7c88d434658bfabdc3d0eb0ba8d |
| Source note | uspto-grants-1997_10 |