HRID1490546
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
CONDITIONS
反应条件
- 温度
- 100 °C
PROCEDURE
实验过程
The general procedure A was followed using 1,3-dimethoxybenzene (65.5 uL, 0.5 mmol) and B2pin2 (126.9 mg, 0.5 mmol, 1.0 eq.) as starting material. The resulting mixture was allowed to stir 16 hours at 100 oC. 5a was obtained as white solid (125.1 mg, 95%) after purification by silica gel flash chromatography (EtOAc/PE=1:30 v/v). m.p.: 87-88 °C