3,4-Dimethylphenol → HCID 164895991, compound

HRID 1490687Notes

Reaction equation

HRID 1490687 reaction equation
Cc1ccc(O)cc1C>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCCCC1.CC(C)(C)c1ccnc(-c2cc(C(C)(C)C)ccn2)c1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.CC1(C)OBOC1(C)C.C[OH2+].C[OH2+].[Ir].[Ir]>Cc1cc(O)c(B2OC(C)(C)C(C)(C)O2)cc1C

Participants

7

Reactant 1

HCID 72493,4-Dimethylphenol

Product 1

HCID 164895991HCID 164895991, compoundYield 68%

Reagents, catalysts & solvents 5

HCID 2733548Bis(pinacolato)diboraneReagentHCID 27347684,4,5,5-Tetramethyl[1,3,2]dioxaborolaneReagentHCID 42491874,4'-Di-tert-butyl-2,2'-bipyridylReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 8078CyclohexaneSolvent

Conditions

Temperature
80 °C

Sources & evidence

ORD record
ord-0981b8908fef4e518b044aef84b80300
Source dataset
Borylation dataset from Roche

Reaction notes

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