2-Methoxy-4-Methylphenol → HCID 129983981, compound

HRID 1490689Notes

Reaction equation

HRID 1490689 reaction equation
COc1cc(C)ccc1O>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCCCC1.CC(C)(C)c1ccnc(-c2cc(C(C)(C)C)ccn2)c1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.CC1(C)OBOC1(C)C.C[OH2+].C[OH2+].[Ir].[Ir]>COc1cc(C)cc(B2OC(C)(C)C(C)(C)O2)c1O

Participants

7

Reactant 1

HCID 71442-Methoxy-4-Methylphenol

Product 1

HCID 129983981HCID 129983981, compoundYield 66%

Reagents, catalysts & solvents 5

HCID 2733548Bis(pinacolato)diboraneReagentHCID 27347684,4,5,5-Tetramethyl[1,3,2]dioxaborolaneReagentHCID 42491874,4'-Di-tert-butyl-2,2'-bipyridylReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 8078CyclohexaneSolvent

Conditions

Temperature
80 °C

Sources & evidence

ORD record
ord-61f3577cdfc140d782ee35ad09fa999f
Source dataset
Borylation dataset from Roche

Reaction notes

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