N,N-dihexylbenzamide → HCID 91820772, compound

HRID 1490826Notes

Reaction equation

HRID 1490826 reaction equation
CCCCCCN(CCCCCC)C(=O)c1ccccc1>C1=CCCC=CCC1.C1=CCCC=CCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.COc1ccc(NC(=O)Nc2ccccc2-c2ccc(-c3ccccn3)nc2)cc1.C[OH2+].C[OH2+].[Ir].[Ir]>CCCCCCN(CCCCCC)C(=O)c1ccc(B2OC(C)(C)C(C)(C)O2)cc1.CCCCCCN(CCCCCC)C(=O)c1cccc(B2OC(C)(C)C(C)(C)O2)c1

Participants

6

Reactant 1

HCID 4577308N,N-dihexylbenzamide

Product 2

HCID 91820772HCID 91820772, compoundYield 13%HCID 140851879HCID 140851879, compoundYield 9%

Reagents, catalysts & solvents 3

HCID 2733548Bis(pinacolato)diboraneReagentHCID 918207751-(2-([2,2'-Bipyridin]-5-yl)phenyl)-3-(4-methoxyphenyl)ureaReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalyst

Conditions

Temperature
25 °C

Sources & evidence

ORD record
ord-3c0973523fb1487eb3b98de7c4448930
Source dataset
Borylation dataset from Roche

Reaction notes

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