HCID 178444788, compound → HCID 91820765, compound

HRID 1490844Notes

Reaction equation

HRID 1490844 reaction equation
CCCCCCN(CCCCCC)C(=O)c1ccccc1C(=O)OC>C1=CCCC=CCC1.C1=CCCC=CCC1.CC(C)(C)c1ccnc(-c2cc(C(C)(C)C)ccn2)c1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc(C)cc1.[Ir].[Ir]>CCCCCCN(CCCCCC)C(=O)c1cc(B2OC(C)(C)C(C)(C)O2)ccc1C(=O)OC

Participants

6

Reactant 1

HCID 178444788HCID 178444788, compound

Product 1

HCID 91820765HCID 91820765, compoundYield 67%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 42491874,4'-Di-tert-butyl-2,2'-bipyridylReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 7809P-XyleneSolvent

Conditions

Temperature
25 °C

Sources & evidence

ORD record
ord-69bb560791764fd58a48ce536994110d
Source dataset
Borylation dataset from Roche

Reaction notes

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