HCID 533309, compound → HCID 91820753, compound

HRID 1490862Notes

Reaction equation

HRID 1490862 reaction equation
CCCCCCN(CCCCCC)C(=O)c1cccc(Br)c1>C1=CCCC=CCC1.C1=CCCC=CCC1.CC(C)(C)c1ccnc(-c2cc(C(C)(C)C)ccn2)c1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc(C)cc1.[Ir].[Ir]>CCCCCCN(CCCCCC)C(=O)c1cc(Br)cc(B2OC(C)(C)C(C)(C)O2)c1

Participants

6

Reactant 1

HCID 533309HCID 533309, compound

Product 1

HCID 91820753HCID 91820753, compoundYield 99%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 42491874,4'-Di-tert-butyl-2,2'-bipyridylReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 7809P-XyleneSolvent

Conditions

Temperature
25 °C

Sources & evidence

ORD record
ord-543c3d6391f9477d91997c2e9ffb8114
Source dataset
Borylation dataset from Roche

Reaction notes

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