HCID 178444794, compound → HCID 91820752, compound

HRID 1490875Notes

Reaction equation

HRID 1490875 reaction equation
CCCCCCN(CCCCCC)C(=O)c1cccn1C>C1=CCCC=CCC1.C1=CCCC=CCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc(C)cc1.O=C(Nc1ccccc1-c1ccc(-c2ccccn2)nc1)NC1CCCCC1.[Ir].[Ir]>CCCCCCN(CCCCCC)C(=O)c1cc(B2OC(C)(C)C(C)(C)O2)cn1C.CCCCCCN(CCCCCC)C(=O)c1ccc(B2OC(C)(C)C(C)(C)O2)n1C

Participants

7

Reactant 1

HCID 178444794HCID 178444794, compound

Product 2

HCID 91820752HCID 91820752, compoundYield 73%HCID 173659682HCID 173659682, compoundYield 11%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 91820779HCID 91820779, compoundReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 7809P-XyleneSolvent

Conditions

Temperature
25 °C

Sources & evidence

ORD record
ord-f898dd206248464eafceb8bc88b048bc
Source dataset
Borylation dataset from Roche

Reaction notes

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