Phosphonic acid, phenyl-, diethyl ester → HCID 57972913, compound

HRID 1490885Notes

Reaction equation

HRID 1490885 reaction equation
CCOP(=O)(OCC)c1ccccc1>C1=CCCC=CCC1.C1=CCCC=CCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc(C)cc1.O=C(Nc1ccccc1-c1ccc(-c2ccccn2)nc1)NC1CCCCC1.[Ir].[Ir]>CCOP(=O)(OCC)c1ccc(B2OC(C)(C)C(C)(C)O2)cc1.CCOP(=O)(OCC)c1cccc(B2OC(C)(C)C(C)(C)O2)c1

Participants

7

Reactant 1

HCID 15642Phosphonic acid, phenyl-, diethyl ester

Product 2

HCID 57660144HCID 57660144, compoundYield 3%HCID 57972913HCID 57972913, compoundYield 49%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 91820779HCID 91820779, compoundReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 7809P-XyleneSolvent

Conditions

Temperature
40 °C

Sources & evidence

ORD record
ord-32d52966647c464e901c99dd1fade510
Source dataset
Borylation dataset from Roche

Reaction notes

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