HCID 12670614, compound → HCID 166609992, compound

HRID 1490887Notes

Reaction equation

HRID 1490887 reaction equation
CCOP(=O)(OCC)c1ccccc1OC>C1=CCCC=CCC1.C1=CCCC=CCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc(C)cc1.O=C(Nc1ccccc1-c1ccc(-c2ccccn2)nc1)NC1CCCCC1.[Ir].[Ir]>CCOP(=O)(OCC)c1cc(B2OC(C)(C)C(C)(C)O2)ccc1OC.CCOP(=O)(OCC)c1ccc(B2OC(C)(C)C(C)(C)O2)cc1OC

Participants

7

Reactant 1

HCID 12670614HCID 12670614, compound

Product 2

HCID 91820766HCID 91820766, compoundYield 28%HCID 166609992HCID 166609992, compoundYield 54%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 91820779HCID 91820779, compoundReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 7809P-XyleneSolvent

Conditions

Temperature
40 °C

Sources & evidence

ORD record
ord-e90dbb04b9a74aa9a72d5b6b22f85339
Source dataset
Borylation dataset from Roche

Reaction notes

Loading…