Diethyl (2-bromophenyl)phosphonate → HCID 91820751, compound

HRID 1490891Notes

Reaction equation

HRID 1490891 reaction equation
CCOP(=O)(OCC)c1ccccc1Br>C1=CCCC=CCC1.C1=CCCC=CCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc(C)cc1.O=C(Nc1ccccc1-c1ccc(-c2ccccn2)nc1)NC1CCCCC1.[Ir].[Ir]>CCOP(=O)(OCC)c1cc(B2OC(C)(C)C(C)(C)O2)ccc1Br.CCOP(=O)(OCC)c1ccc(B2OC(C)(C)C(C)(C)O2)cc1Br

Participants

7

Reactant 1

HCID 284858Diethyl (2-bromophenyl)phosphonate

Product 2

HCID 91820751HCID 91820751, compoundYield 92%HCID 164681383HCID 164681383, compoundYield 7%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 91820779HCID 91820779, compoundReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 7809P-XyleneSolvent

Conditions

Temperature
40 °C

Sources & evidence

ORD record
ord-9bfae5aa6eab4513a48839adbdb839fd
Source dataset
Borylation dataset from Roche

Reaction notes

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