HCID 13549862, compound → HCID 91820782, compound

HRID 1490893Notes

Reaction equation

HRID 1490893 reaction equation
CCOP(=O)(OCC)c1ccccc1C(F)(F)F>C1=CCCC=CCC1.C1=CCCC=CCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc(C)cc1.O=C(Nc1ccccc1-c1ccc(-c2ccccn2)nc1)NC1CCCCC1.[Ir].[Ir]>CCOP(=O)(OCC)c1cc(B2OC(C)(C)C(C)(C)O2)ccc1C(F)(F)F

Participants

6

Reactant 1

HCID 13549862HCID 13549862, compound

Product 1

HCID 91820782HCID 91820782, compoundYield 43%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 91820779HCID 91820779, compoundReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 7809P-XyleneSolvent

Conditions

Temperature
40 °C

Sources & evidence

ORD record
ord-03d161c2ebca4d38abf7e5c2ea224ade
Source dataset
Borylation dataset from Roche

Reaction notes

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