Phosphonic diamide, N,N,N',N'-tetraethyl-P-phenyl- → HCID 91820788, compound

HRID 1490896Notes

Reaction equation

HRID 1490896 reaction equation
CCN(CC)P(=O)(c1ccccc1)N(CC)CC>C1=CCCC=CCC1.C1=CCCC=CCC1.CC(C)(C)c1ccnc(-c2cc(C(C)(C)C)ccn2)c1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc(C)cc1.[Ir].[Ir]>CCN(CC)P(=O)(c1cccc(B2OC(C)(C)C(C)(C)O2)c1)N(CC)CC

Participants

6

Reactant 1

HCID 521174Phosphonic diamide, N,N,N',N'-tetraethyl-P-phenyl-

Product 1

HCID 91820788HCID 91820788, compoundYield 34%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 42491874,4'-Di-tert-butyl-2,2'-bipyridylReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 7809P-XyleneSolvent

Conditions

Temperature
40 °C

Sources & evidence

ORD record
ord-9c37b8d8a8754f95ad15c808224a97c1
Source dataset
Borylation dataset from Roche

Reaction notes

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