HCID 138982594, compound → HCID 91820791, compound

HRID 1490899Notes

Reaction equation

HRID 1490899 reaction equation
COc1ccccc1P(=O)(C1CCCCC1)C1CCCCC1>C1=CCCC=CCC1.C1=CCCC=CCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc(C)cc1.O=C(Nc1ccccc1-c1ccc(-c2ccccn2)nc1)NC1CCCCC1.[Ir].[Ir]>COc1ccc(B2OC(C)(C)C(C)(C)O2)cc1P(=O)(C1CCCCC1)C1CCCCC1

Participants

6

Reactant 1

HCID 138982594HCID 138982594, compound

Product 1

HCID 91820791HCID 91820791, compoundYield 96%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 91820779HCID 91820779, compoundReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 7809P-XyleneSolvent

Conditions

Temperature
25 °C

Sources & evidence

ORD record
ord-aff296fe014348f7b6aca0f8a7eace57
Source dataset
Borylation dataset from Roche

Reaction notes

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