Dicaprylyl Ether → HCID 178443774, compound

HRID 1490984Notes

Reaction equation

HRID 1490984 reaction equation
CCCCCCCCOCCCCCCCC>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCCCCCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc2ccc3cccnc3c2n1.[Ir].[Ir]>CC1(C)OB(CCCCCCCCOCCCCCCCCB2OC(C)(C)C(C)(C)O2)OC1(C)C.CCCCCCCCOCCCCCCCCB1OC(C)(C)C(C)(C)O1

Participants

7

Reactant 1

HCID 12399Dicaprylyl Ether

Product 2

HCID 178431116HCID 178431116, compoundYield 9%HCID 178443774HCID 178443774, compoundYield 43%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 49133562-Methyl-1,10-phenanthrolineReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 9266CyclooctaneSolvent

Conditions

Temperature
100 °C

Sources & evidence

ORD record
ord-ca87645145514f85b26f1107ce24c8c4
Source dataset
Borylation dataset from Roche

Reaction notes

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