Ethyl butyl ether → 2-(2-Butoxyethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

HRID 1490987Notes

Reaction equation

HRID 1490987 reaction equation
CCCCOCC>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCCCCCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc2ccc3cccnc3c2n1.[Ir].[Ir]>CCCCOCCB1OC(C)(C)C(C)(C)O1

Participants

6

Reactant 1

HCID 12355Ethyl butyl ether

Product 1

HCID 860185652-(2-Butoxyethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolaneYield 51%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 49133562-Methyl-1,10-phenanthrolineReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 9266CyclooctaneSolvent

Conditions

Temperature
100 °C

Sources & evidence

ORD record
ord-647d3582d5f54beaab805edca89db85b
Source dataset
Borylation dataset from Roche

Reaction notes

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